Učni načrt predmeta

Predmet:
Sodobni nanostrukturirani kovinski materiali
Course:
Advanced Nanostructured Metallic Materials
Študijski program in stopnja /
Study programme and level		 Študijska smer /
Study field		 Letnik /
Academic year		 Semester /
Semester
Nanoznanosti in nanotehnologije, 3. stopnja / 1 1
Nanosciences and Nanotechnologies, 3rd cycle / 1 1
Vrsta predmeta / Course type
Izbirni
Univerzitetna koda predmeta / University course code:
NANO3-818
Predavanja
Lectures		 Seminar
Seminar		 Vaje
Tutorial		 Klinične vaje
work		 Druge oblike
študija		 Samost. delo
Individ. work		 ECTS
30 30 30 21 10

*Navedena porazdelitev ur velja, če je vpisanih vsaj 15 študentov. Drugače se obseg izvedbe kontaktnih ur sorazmerno zmanjša in prenese v samostojno delo. / This distribution of hours is valid if at least 15 students are enrolled. Otherwise the contact hours are linearly reduced and transfered to individual work.

Nosilec predmeta / Course leader:
izr. prof. dr. Monika Jenko
Sodelavci / Lecturers:
Jeziki / Languages:
Predavanja / Lectures:
Slovenščina, angleščina / Slovene, English
Vaje / Tutorial:
Pogoji za vključitev v delo oz. za opravljanje študijskih obveznosti:
Prerequisites:

Zaključen študij druge stopnje naravoslovne ali tehniške smeri ali zaključen študij drugih smeri z dokazanim poznavanjem osnov področja predmeta (pisna dokazila, pogovor).

Completed second cycle studies in natural sciences or engineering or completed second cycle studies in other fields with proven knowledge of fundamentals in the field of this course (certificates, interview).

Vsebina:
Content (Syllabus outline):

- Znanost o sodobnih nanostrukturiranih kovinskih materialih, biomaterialih, inženiring površin - izbrana poglavja,
- osnove elektronske teorije kovin,
- kristalna struktura kovin,
- napake v kristalih,
- difuzijski procesi v kovinah in zlitinah,
- mehanske lastnosti kovinskih materialov,
- dislokacije in utrjevalni mehanizmi,
- fazni diagrami (osnove),
- fazne spremembe v kovinah, kinetika reakcij v trdnem (nukleacija in rast),
- mikrostruktura kovinskih materialov,
- razvoj kovinske mikrostrukture,
- nanostrukturirani kovinski materiali,
- biokompatibilni kovinski materiali,
- modifikacija površine kovin in zlitin,
- kovinski biomateriali za uporabo v medicini;
biokompatibilnost, mehanska kompatibilnost,
odpornost proti koroziji, tribokoroziji,
- zlitine z oblikovnim spominom, zlitine z
martenzitno fazno premeno; super elastične
zlitine,
- degradacija kovinskih materialov,
- degradacija kovinskih materialov za implantate,
- elektrokemijska korozija, biokorozija,
visokotemperaturna oksidacija.
zlitine izdelane z dodajnimi postopki (AM) oziroma z 3D printanjem
SLM, EBM,
izzivi za poglobljeno razumevanje lastnosti AM novih materialov

- Materials science and engineering of advanced nanstructured metallic materials, biomaterials - selected chapters,
- Basics of Electron theory of metals,
- Crystal structure of Metals,
- Concepts of Crystallography,
- Imperfection in Crystals,
- Diffusion processes in solids - metals and alloys,
- Mechanical properties of metallic materials,
- Dislocations and Strengthening Mechanisms,
- Phase diagrams: Constitution of equilibrium metallic phase diagrams,
- Phase Transformations in Metals the kinetics of solid-state reactions (nucleation, growth),
- Microstructure of metallic materials,
- Development of microstructure of metallic
materials basic aspects,
- Nanostructured metallic materials,
- Biometalic materials,
- Surface modification of metals and alloys,
- Metallic biomaterials for application in medicine; biocompatibility, mechanical compatibility, corrosion resistance, tribo corrosion,
- Shape memory alloys –alloys with martensite
phase transition; super elastic alloys,
- Deagradation of metallic materials,
- Degradation of metallic materials for implants,
- Electrochemical corrosion, biocorrosion,
tribocorrosionhigh temperature oxidation.
AM alloys, manufactured by SLM and EBM procedures
Challenges for deep understanding and applications of the AMed new materials

Temeljna literatura in viri / Readings:

1. Modern Physical Metallurgy R.E. Smallman and A.H.W. Ngan (Eighth Edition) 2014 Elsevier.
2. Physical Metallurgy (Fifth Edition) Edited by:David E. Laughlin and Kazuhiro Hono, 2015 Elsevier.
3. ASTM , Volume 23, Medical and Surgical Materials and Devices, 2012.
4. Degradation of Implant Materials Editors: Eliaz, Noam (Ed.) , Springer 2012.
5. Materials Science and Engineering: Introduction; 6th edition, W.D: Callister, John Willey, 2003).
6. Phase transformation in Metals and alloys 2nd edition, D.a.Porter, K.E. Eastrling (CRC Press, Taylor
Francis group, 2004).
7. Scanning Electron Microscopy and X-ray Microanalysis, J.Goldstein, D. Newbury, D.Joy, Lyman,
P.Echlin, E.Lifshin, L Sawyer and J. Michael, 3rd edition (Cluwer Academic Plenum Publishers, 2003).
8. Surface analysis by AES and XPS, Edts. D.Briggs and J.T.Grant (surface Spectra and Publications 2003).
9. Materials Science and Engineering; 6th edition, W.D: Callister, (John Willey, 2003) 12 F. N. Rhines:
Phase Diagrams in Metallurgy.
10. Robert DeHoff: Thermodynamics in Materials Science, Taylor & Francis, Boca Raton, 2006.
11. Cuie Wen, Editor, Metallic Biomaterials Processing and Medical Device Manufacturing, ISBN: 9780081029657, Woodhead Publishing 2020
12. Shuai Huanga, et al., Progress in additive manufacturing on new materials: A review, Journal of Materials Science &Technology, 35 (2019) 242-269, doi.org/10.1016/j.jmst.2018.09.002
Ciljani izbor in razprava o aktualnih znanstvenih objavah, predvsem v revijah Science, Nature Scientific
reports, Nature Materials, Acta Metallurgica, Acta Biomaterialia Surface Science, Applied Surface Science,
Corrosion science itd. / Targeted selection and discussion of scientific publications, particularly from
Science, Nature, Scientific reports, Nature Materials, Acta Metallurgica, Acta Biomaterialia Surface Science,
Applied Surface Science, Corrosion Science, The Journal of Bone and Joint Surgery." Journal of Materials Science &Technology

Cilji in kompetence:
Objectives and competences:

Cilj predmeta je usposobiti študenta za razumevanje teoretičnega in praktičnega znanja o sodobnih kovinskih materialih, biomaterialih in inženirskih materialih, lastnostih kovinskih materialov, povezanih s strukturo. Cilj se navezuje na kompetence:
- obvladovanje metod in tehnik znanstvenega raziskovanja,
- sposobnost za samostojno in skupinsko raziskovalno in razvojno delo,
- sposobnost uporabe znanja v praksi in
- delno tudi razvoj integralnega načina mišljenja ter sposobnost za komunikacijo s strokovnjaki drugih disciplin in področij.

The objective of the course is to train a student to understand fundamental and applied knowledge of advanced metallic materials, biomaterials and engineering materials, properties of metallic materials and their structures. This objective is related to competences:
- mastering of methods and techniques of scientific research ability to carry out independent as well as team R&D work,
- ability to use the knowledge in practice,
- and partially also to the development of an integral way of thinking and the ability to communicate with experts from other disciplines and fields.

Predvideni študijski rezultati:
Intendeded learning outcomes:

Poznati, razumeti:
procese interakcije atom/površina na atomski
skali, med dinamičnim procesom rasti tanke plasti iz parne faze ali adsorbirane, segregirane tanke plasti, za kontrolirano mikrokemijo, mikrostrukturo in od tod načrtovane fizikalne lastnosti kovinskih materialov.
Poznati in razumeti termodinamiko in kinetiko
razvoja mikrostrukture, konstitucije faznih
diagramov ter temperaturno odvisne lastnosti in
premene v kovinskih materialih.
Poznati in razumeti sodobne kovinske
biomateriale, biokompatibilne in mehansko
kompatibilne kovine in zlitine za uporabo v
medicini.
Poznati in razumeti zlitine z oblikovnim spominom; zlitine z martenzitno premeno.
Poznati in razumeti vmesne površine med
biokompatibilnimi materiali in organskim tkivom.
Poznati osnove biokorozije, karakterizacijo
korozijskih produktov z različnimi preiskovalnimi
metodami za analizo površin.

Know and understand the theory of atom/surface interactions during the dynamic process of vapor- phase or adsorption/ segregation
thin and ultra thin film growth in order to control,
manipulate microchemistry of metallic materials,
microstructure, and, hence, physical properties of
metallic materials.
To know and understand the materials classification and the basics of advanced metallic materials, microstructure evolution of metals and alloys, to know the basic metallurgical thermodynamics and phase diagrams constitution.
To know and understand the temperature
dependent properties and phase transformation of metallic materials.
To know the basics of advanced metallic
biomaterials, bio and mechanical compatibility;
shape memory alloys, materials with martensite
phase transition.
To know and undestand the influence of
biometrials-biointerfaces.
To know the basics of biocorrosion, tribo corrosion and characterization of corrosion products by different methods for surface characterization.

Metode poučevanja in učenja:
Learning and teaching methods:

Uvodna predstavitev.
Seminarsko skupinsko delo.
Vključevanje v projekte za razvoj sposobnosti uporabe opreme.
Uporaba raziskovalne opreme v reševanju izbranega problema, analiza rezultatov, priprava seminarske predstavitve.

Introductory presentation.
Seminar team work.
Participation in projects for the development of ability to use research equipment.
Solving selected problem with research equipment, analysis of results, preparation of the seminar presentation.

Načini ocenjevanja:
Delež v % / Weight in %
Assesment:
Seminarska naloga
50 %
Seminar work
Zagovor seminarske naloge, pri katerem dokaže osvojitev vseh študijskih izidov z vsaj po enim konkretnim primerom
50 %
Defense of the seminar work where the student demonstrates the achievement of all learning outcomes with at least one specific case for each outcome
Reference nosilca / Lecturer's references:
1. JENKO, Monika, GODEC, Matjaž, KOCIJAN, Aleksandra, RUDOLF, Rebeka, DOLINAR, Drago, OVSENIK, Maja, GORENŠEK, Matevž, ZAPLOTNIK, Rok, MOZETIČ, Miran. A new route to biocompatible Nitinol based on a rapid treatment with H 2 / O 2 gaseous plasma. Applied Surface Science, ISSN 0169-4332. [Print ed.], April 2019, vol. 473, str. 976-984, doi: 10.1016/j.apsusc.2018.12.140. [COBISS.SI-ID 21981974],
2. PUKŠIČ, Nuša, JENKO, Monika, GODEC, Matjaž, MCGUINESS, Paul J. A comparison of the uniaxial deformation of copper and nickel (1 1 19) surfaces: a molecular dynamics study. Scientific reports, ISSN 2045-2322, Feb. 2017, vol. 7, str. 1-7, ilustr. http://www.nature.com/articles/srep42234?WT.feed_name=subjects_physics, doi: 10.1038/srep42234. [COBISS.SI-ID 1283498].
3. JENKO, Monika, GORENŠEK, Matevž, GODEC, Matjaž, HODNIK, Maxinne, ŠETINA, Barbara, DONIK, Črtomir, GRANT, John T., DOLINAR, Drago. Surface chemistry and microstructure of metallic biomaterials for hip and knee endoprostheses. Applied Surface Science, ISSN 0169-4332. [Print ed.], Avg. 2017, vol. 427, str. 584-593, ilustr. http://www.sciencedirect.com/science/article/pii/S0169433217323206, doi: 10.1016/j.apsusc.2017.08.007. [COBISS.SI-ID 1331882]
4. AVSEC, Klemen, JENKO, Monika, CONRADI, Marjetka, KOCIJAN, Aleksandra, VESEL, Alenka, KOVAČ, Janez, GODEC, Matjaž, BELIČ, Igor, ŠETINA, Barbara, DONIK, Črtomir, GORENŠEK, Matevž, KOCJANČIČ, Boštjan, DOLINAR, Drago. Surface properties of retrieved cementless femoral hip endoprostheses produced from a Ti6Al7Nb alloy. Coatings, ISSN 2079-6412, December 2019, vol. 9, iss. 12, str., ilustr. https://www.mdpi.com/2079-6412/9/12/868, doi: 10.3390/coatings9120868. [COBISS.SI-ID 1529258]
5. JUAN, J., ORAZI, V., SANDOVAL, M., BECHTHOLD, P., HERNÁNDEZ-LAGUNA, A., SAINZ-DÍAZ, C. I., GONZALES, E. A., JENKO, Monika, JASEN, P. V. DTF study of Ni segregation at B2-NiTi(110)/rutile-TiO2(110) interface. Applied Surface Science, ISSN 0169-4332. [Print ed.], Sept. 2019, vol. 489, str. 287-296, ilustr. https://www.sciencedirect.com/science/article/pii/S0169433219316575. [COBISS.SI-ID 1487786]